请选择 进入手机版 | 继续访问电脑版

乔治   发表于 2018-2-8 13:42:45 |栏目:仪器资料
  • 资料类型 :维护维修 
  • 资源级别: 三星以上
  • 文件类型 : pdf 
  • 适合人群 : 初学者
  • 关联厂家 : 岛津
  • 仪器型号: CLASS-VP
岛津CLASS-VP_Ver.6常见问题解答

索引
1. 安装·············································································································1
问题 1.1. 现有LC-10A Series 单元可以通过 CLASS-VP 控制?·······························1
问题 1.2. 哪些 LC-VP Series 版本号与 CLASS-VP 兼容?········································1
问题 1.3. 哪些 SPD-M10Avp 版本号与 CLASS-VP 兼容?········································1
问题 1.4. CLASS-VP 可以在 Windows NT 下运行吗?···············································1
问题 1.5. 使用软件狗时,CLASS-VP 有时根本不启动或者过了很长时间以后才启
动,这是否说明计算机有问题?·····································································1
问题 1.6. 我的计算机不能与SCL-10Avp(或 LC-2010)正确连接,这可能是什
么原因造成的?································································································1
问题 1.7. 我的计算机偶尔会由于RS-232C 通信错误而死机,有好的对策吗?········1
问题 1.8. 使用 CLASS-VP 控制多个 LC 系统时,SCL-10Avp 和 LC-2010 可以
连接到从市面上买到的任何 RS-232C 插板上吗?·······································2
问题 1.9. 尽管 PDA 检测器已连接到计算机上,但 CLASS-VP 仍无法识别此单
元。···················································································································2
问题 1.10. 在通过SCSI 接口连接 SCL-10Avp 后,此仪器不工作,出了什么问
题?···················································································································2
问题 1.11. 我想在SCL-10Avp 上安装 PC-55N 双通道插板,该怎样设置 DIP 开
关(双列直插式开关)?················································································2
问题 1.12. 我使用的是 PDA 检测器和 Windows NT,然而“PDA Calibration”程序
却无法使用。····································································································3
问题 1.13. 请解释一下如何重新安装CLASS-VP。还有,升级 CLASS-VP 时,是
否有专用的升级磁盘?····················································································3
问题 1.14. 尽管已安装了软件狗,但在打开 CLASS-VP Instrument 窗口时,仍显示
“This file can not be opened in demo mode”这一警告消息。·······················3
问题 1.15. 如果管理员忘记了CLASS-VP 的登录口令,那么初始化 System
Administration 设置的步骤是什么?·······························································3
问题 1.16. 我更换了 LC 单元耗材,该如何重新设置系统检测参数?·························3
问题 1.17. 我更换了PDA 检测器光源,该如何重新设置光源的运行时间?···············4
问题 1.18. 启动 PDA Calibration 时,显示出“Unable to load PdaVp16.dll”这一消
息,出了什么问题?························································································4
问题 1.19. 在一台计算机上可以同时使用CLASS-VP 5.xx 版和 6.0 版吗?···············4
2. 配置·············································································································5
问题 2.1. AutoConfig 可以用来检测和配置 PDA 检测器吗?·····································5
问题 2.2. 检测器Configuration 字段中的 Base Period 的意思是什么?在此应输
入什么值?·······································································································5
一起下吧yqdaw.com
CLASS-VP 常见问题解答 2001/2/28 版
iii
问题 2.3. 尽管可用于 2mL 进样的选配定量管已连接到 LC-2010 自动采样器
上,但不能在 CLASS-VP 软件中将 Injection Volume 值设为大于
100uL。为什么?·····························································································5
问题 2.4. Recycling Valve 可以由 CLASS-VP 6.0 版控制吗?····································5
3. 方法·············································································································6
问题 3.1. 峰处理参数在哪里设置?················································································6
问题 3.2. 峰处理参数的最小面积是如何计算的?·························································6
问题 3.3. 如果在Integration Events Table 的多行中指定了具有相同时间的相同命
令,那么将使用哪一条命令?·········································································6
问题 3.4. [Method] > [Instrument Setup] 菜单的 <System Controller> 选项框中显示
的 Trigger Type 是什么意思?·······································································6
问题 3.5. 在哪里设置 Fraction Collector(馏份收集器)程序?···································6
问题 3.6. 馏份收集器程序有模拟功能吗?·····································································7
问题 3.7. 梯度曲线和馏份收集器程序有图形化设置功能吗?······································7
问题 3.8. 校准曲线类型及其加权方法可以在 Peak 表中选择。也可以在 [Method]
> [Review Calibration Curve] 中选择这些项。两者之间有什么不同?·········7
问题 3.9. Peak 表中有 10 个浓度级别的列。然而极少情况下这 10 个级别都使
用,并且由于存在此 10 列,所以查看该表很困难。··································7
问题 3.10. 如何将数据传输到 EXCEL 中?····································································7
问题 3.11. 如何更改理论塔板数和分离度计算方法?·····················································7
问题 3.12. 我希望自动将数据复制到网络服务器,如何做到这一点?··························7
问题 3.13. 如何进行数据背景补偿?················································································8
问题 3.14. 如何设置 System Suitability(系统适应性)?··············································8
问题 3.15. 可以将 Calibration Curve 的竖轴指定为 Amount 吗?································8
问题 3.16. 请解释一下如何设置和使用方法的Audit Trail(审计跟踪)。···················8
问题 3.17. 一旦激活一个方法的审计跟踪,就再也不能停用,这样很不方便。··········8
问题 3.18. 请解释一下如何将数据转换成 AIA 格式,以及如何导入 AIA 格式的
数据。···············································································································9
问题 3.19. 峰保留时间和面积无法正确传输,这是否因为某些设置不正确?···············9
问题 3.20. 在[Method] > [PDA Setup] 的 General 选项框中设置 Run Time、
Wavelength Range 和 Sampling Period 时出现错误。请解释一下这些参
数之间的关系。································································································9
问题 3.21. 请解释一下[Method] > [PDA Setup] 的 General 选项框中的 Sampling
Frequency (Period) 和 Time Constant 之间的区别。·····································9
问题 3.22. 在[PDA Setup] 的 <Multi-Chromatogram> 选项框中改变了波长和带宽
时,Peak 表中的分析通道将变为另一通道。为什么会出现这种情况?······10
问题 3.23. 峰可以用光谱的 Similarity 标识吗?·····························································10
问题 3.24. 在 [Method] > [Peak/Group Table] 菜单中有一个 Calib Flag 列。此列的
选项有 Average 和 Replace。另外,序列表的 Run Type 列中还有一个
Average Replicates 选项。请解释一下这些项之间的联系。·························10
问题 3.25. 请解释一下如何通过相对保留时间设置已命名的峰。··································12
一起下吧yqdaw.com
CLASS-VP 常见问题解答 2001/2/28 版
iv
4. 自动进样器程序···························································································13
问题 4.1. 如何编辑预处理程序?····················································································13
问题 4.2. 自动进样器程序设置窗口包含 Dilution 和 Reagent 选项。这些功能可
在 SIL-10A 或 SIL-10AXL 中使用吗?在 SCL-10Avp 上,这些功能好
像只能用于 SIL-10ADvp。·············································································13
问题 4.3. 对建立自动进样器预处理程序有什么限制吗?··············································13
5. 分析·············································································································14
问题 5.1. 每次启动软件时都要登录有点太麻烦。请解释一下如何禁用登录功能。···14
问题 5.2. 如何执行斜率测试?························································································14
问题 5.3. 使用色谱图屏幕的弹出菜单的[Graphical Programming] 菜单项中的
[SLOPE] 执行斜率测试时,有时会出现“Not enough points for SLOPE
calculation. Please select a longer time interval.”这一消息。应如何确定时
间周期?···········································································································14
问题 5.4. 请解释一下开始运行前应如何监视基线。·····················································14
问题 5.5. 当用手动进样器注入样品时,SCL-10Avp 开始执行 Run。然而,
CLASS-VP 只显示一个要求开始采集数据的信息框,但并不执行采集。···14
问题 5.6. 我的系统中有一个二极管阵列检测器 (SPD-M10Avp)。当触发器类型设
为 External 并执行 Run 时,SCL-10Avp 执行 Run,但 CLASS-VP 并
不开始采集数据。而当触发器类型设为 Manual 时,没有任何问题。·······15
问题 5.7. 可以显示梯度曲线吗?····················································································15
问题 5.8. 执行 Run 时,如果已存在一个同名的数据文件,将会显示一条错误消
息而且 Run 不启动。应如何覆盖数据文件?···············································15
问题 5.9. 即使 USP Width 已指定为一个色谱图注释项,但在注释字段中只显示
为 0。另外,USP Width 的切线则无法显示。·············································15
问题 5.10. 尽管二极管阵列检测器 (SPD-M10Avp) 工作正常,但无法通过 direct
control(直接控制)来打开和关闭光源。······················································15
问题 5.11. 显示 PDA 等高线图时,需要很长时间才显示出绘制的图形。···················15
问题 5.12. 在 PDA Mixed View 中,用鼠标右键单击光谱屏幕以显示弹出菜单,但
无法使用 Operation 或 Calc Lambda-max.. 菜单项。··································16
问题 5.13. 在 PDA Mixed View 中,如何向 Similarity 表中添加光谱图? ·················16
问题 5.14. 在 PDA Mixed View 中,纯度曲线和峰轮廓图无法显示。·························16
问题 5.15. 在 PDA Mixed View 中,如何从色谱图窗格中选择光谱或从光谱窗格中
选择波长?·······································································································16
问题 5.16. 尽管 SCL-10Avp 状态已变为“Run”,CLASS-VP 还是不启动数据采
集。···················································································································16
问题 5.17. 按下 [Preview] 按钮时,显示出“All channels are off. No acquisition will
be performed”这一消息,出现了什么错误?················································16
问题 5.18. 如何改变数据图的 Y 轴标尺?······································································16
6. 序列·············································································································17
问题 6.1. 编辑一个序列时,我希望让数据文件名自动递增,比如“TEST01”、
“TEST02”... 如何做到这一点?····································································17
一起下吧yqdaw.com
CLASS-VP 常见问题解答 2001/2/28 版
v
问题 6.2. 我使用 [File] > [Sequence] > [New] 命令创建了下面这样一个表: Data
file: TEST Start vial number: 0 End vial number: 0 Repetitions per run:
2 当执行 Sequence Run 时,数据文件将以什么名称保存?····················17
问题 6.3. 使用 [File] > [Sequence] > [New] 命令进行了下面的设置: Data file:
TEST Start vial number: 0 End vial number: 0 Repetitions per run: 2
选中“Repetitions create multiple records.”复选框。在这种情况下,
表的数据文件名会是什么?·············································································17
问题 6.4. 编辑一个序列时,Clear All Calibration 和 Clear Calibration at Level 这两
种运行类型之间的区别是什么?·····································································17
问题 6.5. 分类校准的 Standard、Std /w Clear Calib 和 Sequence 之间有什么区别?··18
问题 6.6. 执行样品序列时,未生成摘要报告,应如何设置?······································19
问题 6.7. 即使在使用 UV 检测器的双波长模式或使用 PDA 检测器的多谱图数
据时,也可以创建摘要报告吗?·····································································19
问题 6.8. 执行一个样品序列时,未创建此序列的校准报告,应如何设置它?···········19
问题 6.9. 执行一个样品序列时,未创建此序列的 Duplicate(平行)报告,应如何
设置它?···········································································································19
问题 6.10. 执行一个样品序列时,未创建此序列的 Spike(回收率)报告,应如何
设置它?···········································································································20
问题 6.11. 执行一个样品序列时,未创建此序列的 Check Std(控制样)报告,应
如何设置它?····································································································20
问题 6.12. 执行一个样品序列时,未创建此序列的 System Suitability(系统适应
性)报告,应如何设置它?·············································································20
问题 6.13. 如何在序列 Run Type 列表中使用 Shut Down (SHD) 选项?·····················20
问题 6.14. 如何使用 Action 设置的 Test 组合框中的 Hardware Status 选项?··········21
问题 6.15. 如果所有要同时测量的组分未包含在一个标准溶液中,则应如何设置
Peak 表和序列?······························································································21
问题 6.16. 当在一个序列的 Action 功能中指定 Reinject 时,没有地方可输入新的
数据文件名。执行此功能时,原有数据会被覆盖吗?··································21
问题 6.17. 尽管在一个序列中已选择了 Bracketing 模式,标样数据仍未用作校准数
据。···················································································································21
问题 6.18. 推荐哪一版本的 MS-EXCEL 用于 Sequence Wizard?································21
7. 报告·············································································································23
问题 7.1. 执行 Run 时,未创建报告。应如何设置方法报告?···································23
问题 7.2. [Method] > [Custom Report] 与 [Sequence] > [Custom Report] 之间有何区
别?···················································································································23
问题 7.3. 可以将梯度曲线输出到报告中吗?···································································23
问题 7.4. 指定 PDA 多色谱图通道时,如何查看标准报告,如 Area% 报告?········23
问题 7.5. 输出报告时,有时会出现 BDL。这说明什么问题?····································23
问题 7.6. 当方法的 [Custom Report] 中包括 Library Search Results 时,只打印出
表的标题。·······································································································23
问题 7.7. 色谱图和表可以并排打印吗?········································································24
一起下吧yqdaw.com
CLASS-VP 常见问题解答 2001/2/28 版
vi
问题 7.8. 两个图形(如色谱图)可以用完全相同的格式打印并横向排列吗?···········24
问题 7.9. 菜单项 [File] > [Report Template] > [Open] 为灰色,所以无法打开报告
模板。···············································································································24
问题 7.10. 如何删除已插入到 Custom Report 中的图形(如校准曲线)?··················24
问题 7.11. 选择 [Report] > [View / Print]) > [Sequence Custom Report] 时不显示报
告。···················································································································24
问题 7.12. 如何在 Custom Report 中插入分页符?·························································24
问题 7.13. 报告模板文件有三种扩展名:REP、SRP 和 BRP。它们有何区别?·········25
问题 7.14. 当在 [Method] > [PDA Setup] 的 <Multi-chromatogram> 选项框中改变
了通道波长和(或)带宽时,报告中不打印色谱图。··································25
问题 7.15. 当色谱图图形显示在 Custom Report 中时,图形轴上的值和峰注释中的
字符不可读,即使改变字体,也还是一样。··················································25
问题 7.16. Similarity Index 值在 Custom Report 中变成了 0,应该怎样设置它?········25
问题 7.17. 如何初始化 Custom Report(定制报告)设置?···········································25
问题 7.18. 如何将Run Report(运行报告)变成十进制数?·········································25
8. POST RUN 分析··························································································26
问题 8.1. 在 Offline Processing 和 Instrument 1 to 4 窗口中都可以执行Post Run
分析。这之间有什么区别?·············································································26
问题 8.2. 我在 Offline Processing 窗口中选择 Instrument 1 to 4。那么当我选择
[File] > [Data] > [Open] 并选中 Open With Method 时,仪器的方法也会
改变吗?···········································································································26
问题 8.3. 是否有一种 Chromatopac Integration Events 的手动处理功能?···················26
问题 8.4. 如何对两个色谱图相减得到的新色谱图进行分析?······································26
9. 其他项·········································································································27
问题 9.1. CLASS-LC10 的色谱图文件可以直接读入 CLASS-VP。在 CLASSLC10
中应如何读取 CLASS-VP 色谱图数据?············································27
问题 9.2. 可以对用 CLASS-VP 采集到的数据进行 GPC 计算吗? ···························27
问题 9.3. 仪器、方法和数据名称显示在标题栏内。在方法名旁边,有时会显示
Read-only。为什么? ·······················································································27
问题 9.4. 在 <System Administration> 菜单中选择 Purchased Options 时,将显示
产品系列号,这说明什么问题?·····································································27
问题 9.5. 我希望在 Run 期间直接向 MO 或可拆卸的磁盘中写入数据。·················27
问题 9.6. 绘制等高线图和三维谱图过程中可以取消绘制吗?······································27
问题 9.7. 怎样才能删除 Instrument Activity Log?························································28
问题 9.8. 从 Spectrum 窗口的弹出菜单中选择 [Library Search] > [Use Method
Parameter] 时,未执行 Library Search(谱库搜索)。·································28
问题 9.9. 怎样才能将色谱图和光谱图形粘贴到 Microsoft Word 中?························28
问题 9.10. 怎样才能将等高线图和 3D 图形粘贴到 Microsoft Word 中?····················28
请点击此处下载

请先注册会员后在进行下载

已注册会员,请先登录后下载

提取码:p7ou 
下载次数:1    状态:您未购买  售价:5℃
下载权限: 氦级  以上或 提升等级 [充铜板] [兑话费] [发资源赚铜板]  [赚℃值]



上一篇:Agilent1200系列二级管阵列和多波长紫外检测器用户手册
下一篇:HPLC:A Practical User’s Guide HPLC的使用指南(英文原版电子书)

发帖前要善用【论坛搜索】功能,以免资源重复发布;

如果吧里没有您要寻找的资源,请在【求资源】版面发帖求助,得到应助请及时结帖;

如何回报帮助你的吧友,一个好办法就是给对方【顶帖】,顶帖不加分不扣分,但可以让对方的帖子靠前让更多的人看到!

回复 显示全部楼层 使用道具 举报

microsea

氦级

microsea   发表于 2018-2-10 18:19:10 |栏目:仪器资料
啥也不说了,感谢一起下吧和楼主的分享哇!

发帖前要善用【论坛搜索】功能,以免资源重复发布;

如果吧里没有您要寻找的资源,请在【求资源】版面发帖求助,得到应助请及时结帖;

如何回报帮助你的吧友,一个好办法就是给对方【顶帖】,顶帖不加分不扣分,但可以让对方的帖子靠前让更多的人看到!

rprrp

氦级

rprrp   发表于 2018-2-12 18:41:41 |栏目:仪器资料
额,為神馬現在才發現一起下吧的資源啊[email protected][email protected]

发帖前要善用【论坛搜索】功能,以免资源重复发布;

如果吧里没有您要寻找的资源,请在【求资源】版面发帖求助,得到应助请及时结帖;

如何回报帮助你的吧友,一个好办法就是给对方【顶帖】,顶帖不加分不扣分,但可以让对方的帖子靠前让更多的人看到!

jy02717049

氦级

jy02717049   发表于 2018-2-14 22:42:40 |栏目:仪器资料
我帶著醬油瓶路過一起下吧的,還是忍不住小手一抖!

发帖前要善用【论坛搜索】功能,以免资源重复发布;

如果吧里没有您要寻找的资源,请在【求资源】版面发帖求助,得到应助请及时结帖;

如何回报帮助你的吧友,一个好办法就是给对方【顶帖】,顶帖不加分不扣分,但可以让对方的帖子靠前让更多的人看到!

yarbang

氦级

yarbang   发表于 2018-2-17 12:42:41 |栏目:仪器资料
珍惜生命,果断回帖;酌一杯清茶,品一起下吧资源

发帖前要善用【论坛搜索】功能,以免资源重复发布;

如果吧里没有您要寻找的资源,请在【求资源】版面发帖求助,得到应助请及时结帖;

如何回报帮助你的吧友,一个好办法就是给对方【顶帖】,顶帖不加分不扣分,但可以让对方的帖子靠前让更多的人看到!

ihobo

氦级

ihobo   发表于 2018-2-20 15:27:30 |栏目:仪器资料
啥也不说了,感谢一起下吧和楼主的分享哇!

发帖前要善用【论坛搜索】功能,以免资源重复发布;

如果吧里没有您要寻找的资源,请在【求资源】版面发帖求助,得到应助请及时结帖;

如何回报帮助你的吧友,一个好办法就是给对方【顶帖】,顶帖不加分不扣分,但可以让对方的帖子靠前让更多的人看到!

ononpig

氦级

ononpig   发表于 2018-2-23 04:12:18 |栏目:仪器资料
么有分,谁能送我点搬砖数值啊::>_<::

发帖前要善用【论坛搜索】功能,以免资源重复发布;

如果吧里没有您要寻找的资源,请在【求资源】版面发帖求助,得到应助请及时结帖;

如何回报帮助你的吧友,一个好办法就是给对方【顶帖】,顶帖不加分不扣分,但可以让对方的帖子靠前让更多的人看到!

leiing

氦级

leiing   发表于 2018-2-25 04:10:28 |栏目:仪器资料
么有分,谁能送我点搬砖数值啊::>_<::

发帖前要善用【论坛搜索】功能,以免资源重复发布;

如果吧里没有您要寻找的资源,请在【求资源】版面发帖求助,得到应助请及时结帖;

如何回报帮助你的吧友,一个好办法就是给对方【顶帖】,顶帖不加分不扣分,但可以让对方的帖子靠前让更多的人看到!

jiefy

氦级

jiefy   发表于 2018-2-27 04:03:35 |栏目:仪器资料
這麼好的帖子都沒有人頂!d=====( ̄▽ ̄*)b,我來多頂頂樓主

发帖前要善用【论坛搜索】功能,以免资源重复发布;

如果吧里没有您要寻找的资源,请在【求资源】版面发帖求助,得到应助请及时结帖;

如何回报帮助你的吧友,一个好办法就是给对方【顶帖】,顶帖不加分不扣分,但可以让对方的帖子靠前让更多的人看到!

moonfo

氦级

moonfo   发表于 2018-3-1 00:33:18 |栏目:仪器资料
這個資源非常需要,支持一起下吧!

发帖前要善用【论坛搜索】功能,以免资源重复发布;

如果吧里没有您要寻找的资源,请在【求资源】版面发帖求助,得到应助请及时结帖;

如何回报帮助你的吧友,一个好办法就是给对方【顶帖】,顶帖不加分不扣分,但可以让对方的帖子靠前让更多的人看到!

您需要登录后才可以回帖 登录 | 立即注册

本版积分规则

作者相关信息

极品资源推荐

热门资源推荐

最新资源推荐

高分悬赏

热门Tag标签

 
 
在线客服
广告服务
工作时间:
8:00-22:00
客服QQ:
1197719870
关注官方微信公众号
快速回复 返回顶部 返回列表