核磁共振电子书：《the basics of nmr》 (Joseph P. Hornak, Ph.D.)

仪器资料 · 发表于 2018-7-20 17:51:30

Preface (Help)
About the author
Introduction
NMR
NMR Spectroscopy
Units Review

The Mathematics of NMR
Exponential Functions
Trigonometric Functions
Differentials and Integrals
Vectors
Matrices
Coordinate Transformations
Convolutions
Imaginary Numbers
The Fourier Transform

Spin Physics
Spin
Properties of Spin
Nuclei with Spin
Energy Levels
NMR Transitions
Energy Level Diagrams
Continuous Wave NMR Experiment
Boltzmann Statistics
Spin Packets
T1 Processes
Precession
T2 Processes
Rotating Frame of Reference
Pulsed Magnetic Fields
Spin Relaxation
Spin Exchange
Bloch Equations

NMR Spectroscopy
Chemical Shift
Spin-Spin Coupling
Time Domain NMR Signal
+/- Frequency Convention

Fourier Transforms
Introduction
The + and - Frequency Problem
The Fourier Transform
Phase Correction
Fourier Pairs
The Convolution Theorem
The Digital FT
Sampling Error
The Two-Dimensional FT

Pulse Sequences
Introduction
90-FID
Spin-Echo
Inversion Recovery

NMR Hardware
Hardware Overview
Magnet
Field Lock
Shim Coils
Sample Probe
RF Coils
Gradient Coils
Qadrature Detector
Digital Filtering
Safety

Practical Considerations
Introduction
Sample Preparation
Exchange
Probe Tuning
Determining a 90o Pulse
Field Shimming
Phase Cycling
1-D Hydrogen Spectra
Integration
SNR Improvement
Variable Temperature
Troubleshooting
Cryogen Fills
Unix Primer

Carbon-13 NMR
Introduction
Decoupling
Population Inversion
NOE
1-D Spectra

2-D Techniques
Introduction
J-resolved
COSY
Examples

Advanced Spectroscopic Techniques
Introduction
Diffusion
Spin Relaxation Time
Solid State
Microscopy
Solvent Suppression

Glossary
List of Symbols
References
Usage Statistics
Software License